Y-PSZ/Bioglass 45S5 composite obtained by the infiltration technique of porous pre-sintered bodies using sacrificial molding

Authors

DOI:

https://doi.org/10.33448/rsd-v10i7.16920

Keywords:

5Y-PSZ; Bioglass 45S5; 3D printing; Composite; Infiltration; Characterizations.

Abstract

The aim of this work was to obtain porous ceramic parts based on Zirconia stabilized with 5mol.% Yttria (5Y-PSZ), suitable for the infiltration with bioactive glasses, using 3D printed sacrificial polymeric molds. In a first step, honeycomb structured molds were designed with the SolidWorks® software and manufactured by 3D printing using polylactic acid filaments (PLA). These molds were filled with a ceramic mass composed of 5Y-PSZ nanoparticles containing 3wt% polymeric binder and consolidated under pressure of 10MPa and then sintered at 1200 °C-30 min the polymeric molds were consumed. The obtained hexagonal-shaped, porous 5Y-TZP bodies were infiltrated with the bioactive glass 45S5, calcium sodium phosphosilicate, at 1350 °C. The materials were characterized by their relative density, their phase composition by X-ray diffraction analysis, and their microstructure by scanning electron microscopy (SEM-EDS), besides their mechanical properties of hardness and fracture toughness. Pre-sintered 5Y-PSZ substrates exhibit relative density around 75%, and 90% after sintering and Bioglass infiltration. The samples' microstructure is composed of a 5Y-PSZ matrix of sub-micrometric zirconia grains with an average size of 1.0 mm, besides the secondary infiltrated glassy phase homogeneously distributed, with a Ca/P ratio of 1.7, close to the ideal proportion for hydroxyapatite formation. In conclusion, sacrificial molding is an interesting route to obtaining dense Y-PSZ/Bioglass 45S5 composite in a honeycomb format.

References

Agarwala, M. K., Jamalabad V. R., Langrana N. A., Safari. A., Whalen P. J., & Danforth, (1996), Structural quality of parts processed by fused deposition, Rapid Prototyping Journal, 2(4), 4-19.

Alves, M. F. R. P., Ribeiro, S., Suzuki, P. A., Strecker, K., & Santos, C. (2021) Effect of Fe2O3 Addition and Sintering Temperature on mechanical Properties and Translucence of Zirconia Dental Ceramics with Different Y2O3 Content, Materials Research. 24(2): e20200402

Amarante, J. E. V., Pereira, M. V. S., Souza, G. M., Alves, M. F. R. P., Simba, B. G., & Santos, C. (2018) Roughness and its effects on flexural strength of dental yttria-stabilized zirconia ceramics. Materials Science and Engineering: A., 739, 149-157.

Baino F., & Fiume, E., (2019) Elastic Mechanical Properties of 45S5-Based Bioactive Glass–Ceramic Scaffolds, Materials, 12, 3244.

Baino, F., Hamzehlou, S., & Kargozar, S. (2018) Bioactive glasses: Where are we and where are we going? J. Funct. Biomater., 9, 25.

Campana, V., Milano, G., Pagano, E., Barba, M., Cicione, C., Salonna, G., Lattanzi, W., & Logroscino, G. (2014) Bone substitutes in orthopaedic surgery: From basic science to clinical practice. J. Mater. Sci. Mater. Med.., 25, 2445–2461.

Camposilvan, E., Leone, R., Gremillard, L., Sorrentino, R., Zarone, F., Ferrari, M., & Chevalier J. (2018) Aging resistance, mechanical properties and translucency of different yttria-stabilized zirconia ceramics for monolithic dental crown applications, Dental Materials, 34(6) 879-890.

Daguano, J. K. M. F., Rogero, S. O., Crovace, M. C., Peitl, O., Strecker, K., & Santos, C., (2013) Bioactivity and cytotoxicity of glass and glass–ceramics based on the 3CaO·P2O5–SiO2–MgO system, Journal of Materials Science: Materials in Medicine , 24, 2171–2180.

Gibson, I., Rosen, D. W., & Stucker, B. (2010) Additive Manufacturing Technologies: Rapid Prototyping to Direct Digital Manufacturing, Springer Science+Business Media, New York, 459p.

Guo, X., & He, J. (2003), Hydrothermal degradation of cubic zirconia, Acta Materialia, 51 17, 5123-5130.

Hench, L. L. (1991) Bioceramics: From concept to clinic. J. Am. Ceram. Soc. 74, 1487–1510.

Hoppe, A., Güldal, N. S., & Boccaccini, A. R. (2011) A review of the biological response to ionic dissolution products from bioactive glasses and glass-ceramics. Biomaterials, 32, 2757–2774.

Jones, J. R., Brauer, D. S., Hupa, L., & Greenspan, D. C. (2016) Bioglass and bioactive glasses and their impact on healthcare. Int. J. Appl. Glass Sci., 7, 423–434.

Juraski, A. C., Figueiredo, D. C., Daghastanli N. A., Santos, C., Fernandes, M. H. V., da Ana, P. A., & Daguano J. K. M. B. (2021) Effect of a whitlockite glass-ceramic on the occlusion of dentinal tubules for dentin hypersensitivity treatment, Research, Society and Development, 10 (3), e19610313161

Karakurt I., & Lin, L., (2020) 3D printing technologies: techniques, materials, and post-processing, Current Opinion in Chemical Engineering, 28, 134-143

Kim, H. S., Kumbar, S. G., & Nukavarapu, S. P. (2021), Review: Biomaterial-directed cell behavior for tissue engineering, Current Opinion in biomedical engineering, 17, 100260

Rahaman, M. N., Day, D. E., Bal, B. S., Fu, Q., Jung, S. B., Bonewald, L. F., & Tomsia, A. P. (2011) Bioactive glass in tissue engineering. Acta Biomater., 7, 2355–2373.

Prasad, S., Vyas, V. K., Ershad, M. D., & Pyare, R. (2017) Crystallization and mechanical properties of (45S5-HA) biocomposite for implantation , Ceramics-Silikáty 61 (4), 378-384

Reveron, H., & Chevalier, J. (2021), Yttria-stabilized zirconia as a biomaterial: from orthopedic towards dental applications, Encyclopedia os materials technical ceramics and glasses, 3, 540-552.

Zhou M. Y., Xi, J. T., & Yan, J. Q. (2004) Adaptive direct slicing with non-uniform cusp heights for rapid prototyping. Int J Adv Manuf Technol 23(1–2):20–27.

Downloads

Published

25/06/2021

How to Cite

LUZO, R. de O.; OLIVEIRA, V. D. de; COSTA, M. A. da; SANTOS, C. dos; AMARANTE, J. E. V.; DAGUANO, J. K. M. B. .; STRECKER, K.; ALVES, M. F. R. P. Y-PSZ/Bioglass 45S5 composite obtained by the infiltration technique of porous pre-sintered bodies using sacrificial molding. Research, Society and Development, [S. l.], v. 10, n. 7, p. e57510716920, 2021. DOI: 10.33448/rsd-v10i7.16920. Disponível em: https://rsdjournal.org/index.php/rsd/article/view/16920. Acesso em: 23 nov. 2024.

Issue

Vol. 10 No. 7

Section

Engineerings

License

Copyright (c) 2021 Raphael de Oliveira Luzo; Vinícios Dias de Oliveira; Marco Antonio da Costa; Claudinei dos Santos; José Eduardo Vasconcellos Amarante; Juliana Kelmy Macário Barboza Daguano; Kurt Strecker; Manuel Fellipe Rodrigues Pais Alves

Creative Commons License

This work is licensed under a Creative Commons Attribution 4.0 International License.

Authors who publish with this journal agree to the following terms:

1) Authors retain copyright and grant the journal right of first publication with the work simultaneously licensed under a Creative Commons Attribution License that allows others to share the work with an acknowledgement of the work's authorship and initial publication in this journal.

2) Authors are able to enter into separate, additional contractual arrangements for the non-exclusive distribution of the journal's published version of the work (e.g., post it to an institutional repository or publish it in a book), with an acknowledgement of its initial publication in this journal.

3) Authors are permitted and encouraged to post their work online (e.g., in institutional repositories or on their website) prior to and during the submission process, as it can lead to productive exchanges, as well as earlier and greater citation of published work.