Holdup and characteristic velocity in a pulsed packed extraction column

Authors

DOI:

https://doi.org/10.33448/rsd-v9i8.2543

Keywords:

Pulsed packed extractor; Hydrodynamic; Dispersed phase holdup; Characteristic velocity.

Abstract

The present work aims to evaluate the hydrodynamics of a pulsed packed extractor, with an internal diameter of 0.026m and a length of 1.0m, using the liquid butanol-water system. Thus, the basic parameters obtained for the hydrodynamic study of the extraction column in question as dispersed phase, slip velocity, characteristic velocity and flooding point. The methodology used in the work consisted of determining the holdup fraction of the dispersed phase, obtained through tests of simultaneous interruptions in the column feedings. The effects of frequency pulsation, dispersed phase flow rate and continuous phase flow rate investigated in the analysis of these parameters. New empirical correlations derived from the predictions of the parameters studied obtained in terms of operating variables and physical properties of the liquid system involved. The average absolute value of the relative error (AARE) was always below 5.6%. Good agreement between calculated and experimental results observed for all investigated operating conditions.

Author Biographies

Jarlon Conceição da Costa, Universidade Federal da Bahia

PPEQ/UFBA

Luiz Mário Nelson de Góis, Universidade Salvador

EAETI/UNIFACS/SALVADOR/BAHIA

Silvana Mattedi e Silva, PPEQ/UFBA

PPEQ/UFBA

References

Coimbra, S. R., Mojola, F., & Meirelles, J. A. (1998) Dispersed phase holdup in a perforated rotating disk contactor, Journal Chemical Engineering Japan, 31(1), 277–280.

Gayler, R., & Pratt, H. R. C. (1951). Holdup and pressure drop in packed columns, Chemical Engineering Research and Design (Trans IChemE), 29(1), 110

Gholam Samani, M., Haghighi Asl, A., Safdari, J., & Torab-Mostaedi, M., (2012). Drop size distribution and mean drop size in a pulsed packed extraction column, Chemical Engineering Research and Design, 90(1), 2148-2154

Hanley, E. J., & Seader, J. D., (1981). Equilibrium-stage separation operations in chemical engineering, 5rd. John Wiley & Sons, New York

Treybal, R. E., Liquid Extraction. (McGraw Hill Pub. Co, New York) (1963)

Kumar, A., Stelner, L., & Hartland, S., (1986).Capacity and hydrodynamics of an agitated extraction column, Industrial & Engineering Chemistry Process Design and Development, 25(3): 728–733

Kumar, A., & Hartland, S., (1988). Prediction of dispersed phase holdup and flooding velocities in Karr reciprocating plate extraction columns, Industrial & Engineering Chemistry Research, 27, 132–138

Kumar, A., & Hartland, S., (1994).Prediction of drop size, dispersed phase holdup, slip velocity and limiting throughputs in packed extraction columns, Chemical Engineering Research and Design, 72, 89–104

Kumar, A., & Hartland, S., A unified correlation for the prediction of dispersed phase holdup in liquid–liquid extraction columns, Industrial & Engineering Chemistry Research, 34, 3925–3939 (1995).

Mısek, T., Berger, R., & Schroter, (1978). J., Recommended systems for liquid extraction studies. (European Federation of Chemical Engineering, Institution of Chemical Engineers, Rugby)

Napeida, M., Haghighi Asl, A., Safdari, J., Torab-Mostaedi. M., (2010) Holdup and characteristic velocity in a Hanson mixer-settler extraction column, Chemical Engineering Research and Design, 88, 703–711.

Ousmane, S., Isabelle, M., Mario, M. S., Mamadou, T., Jacques, A., Study of mass transfer and determination of drop size distribution in a pulsed extraction column, Chemical Engineering Research and Design, 89 (1), 60-68 (2011).

Richardson, J. F. and Zaki, W. N., (1954).Sedimentation and Fluidisation, part I, Transactions of the Institution of Chemical Engineers, 32, 35-53

Seader, J. D., Henley, E. J., (2006), Separation Process Principles. New York: John WIley and Sons (Asis), 756 p. ISBN 047586269 (enc.).

Simons, A. J. F. I (1983) Handbook of Solvente Extraction. T. C. Lo, M. H. I. Baird, C. Hanson, Eds. John Wiley e Sons. New York, NY, 343-353.

Thornton, J. D., (1956).Spray liquid–liquid extraction columns: prediction of limiting holdup and flooding rates, Chemical Engineering Science, 5(5), 201–208

Torab-Mostaedi, M., Safdari, J., Moosavian, M. A., Ghannadi Maragheh, M., (2009) Stage efficiency of Hanson mixer–settler extraction column, Chemical Engineering and Processing, 48(1), 224–228).

Torab-Mostaedi, M., Ghaemi, A., Asadollahzadeh, (2011).M., Flooding and drop size in a pulsed disc and doughnut extraction column, Chemical Engineering Research and Design, 8(12), 2742-2751

Van Dijck, W. (1935).IO, US. Patent 2,001, 1986

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Published

28/07/2020

How to Cite

COSTA, J. C. da; GÓIS, L. M. N. de; SILVA, S. M. e. Holdup and characteristic velocity in a pulsed packed extraction column . Research, Society and Development, [S. l.], v. 9, n. 8, p. e674982543, 2020. DOI: 10.33448/rsd-v9i8.2543. Disponível em: https://rsdjournal.org/index.php/rsd/article/view/2543. Acesso em: 25 apr. 2024.

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Section

Engineerings