Influence of different surface treatment protocols on the bond strength of itrite stabilized polycrystalline zirconia Itry stabilized polycrystalline tetragonal
DOI:
https://doi.org/10.33448/rsd-v9i12.10921Keywords:
Ceramic; Y-TZP Ceramic; Shear Strength; Resin Cements; Hydrofluoric Acid.Abstract
Evaluate the influence of different surface treatment protocols on shear bond strength in zirconia ceramics. A hundred zirconia cylinders were made using a CAD/CAM system. The specimens were divided into 10 groups: No treatment; Clearfil Ceramic Primer; Scotch bond Universal; Clearfil Ceramic Primer + Scotch bond Universal; 50% hydrofluoric acid + Scotch bond Universal; Airborne-particle abrasion; Airborne-particle abrasion + Clearfil Ceramic Primer; Airborne-particle abrasion + Scotch bond Universal; Airborne-particle abrasion + Clearfil Ceramic Primer + Scotch bond Universal; Airborne-particle abrasion+50% hydrofluoric acid + Scotch bond Universal. All specimens were cemented with Panavia F 2.0, stored in distilled water, and then thermo cycled. The shear bond strength test was performed in a universal testing machine. Fractographic and surface zirconia analysis was done with a stereomicroscope, SEM and WDS. Data were analyzed using Pearson’s chi-square test, Fisher exact test, and the Kruskal-Wallis test. The highest shear bond strength values were observed in the groups treated with hydrofluoric acid, besides, these groups did not show pre-test failure. The predominant failure mode was adhesive. Among the surface treatment protocols evaluated, 50% hydrofluoric acid conditioning associated with the Scotchbond Universal adhesive system offers higher values of shear bond strength to the zirconia, regardless of the use of microblasting.
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Copyright (c) 2020 Leonardo José Rodrigues de Oliveira; Monica Soares de Albuquerque; Armiliana Soares Nascimento; Cacio Mendes; Paulo de Assis; Luan Bernardo; Rodivan Braz
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