Síntese e caracterização de uma cerâmica dentária experimental 3Y-TZP preparada pelo método de precursores poliméricos

Autores

DOI:

https://doi.org/10.33448/rsd-v9i10.9123

Palavras-chave:

Cerâmica; 3Y-TZP; Síntese Química; Termogravimetria; Difração de raios X; Microscopia eletrônica de varredura.

Resumo

O objetivo da pesquisa foi sintetizar pós de zircônia estabilizada com 3 mol% de ítria (3Y-TZP) por meio do método de precursores poliméricos (MPP). A solução precursora foi pré-aquecida a 350ºC por 3h, posteriormente tratada termicamente a 500ºC por 3h e 800ºC por 6h. Os materiais obtidos foram analisados por Termogravimetria – Termogravimetria Derivada (TG / DTG), Análise Térmica Diferencial (DTA), Difração de raios-X (DRX) e Microscopia Eletrônica de Varredura (MEV). Dois sistemas cerâmicos Y-TZP comercialmente disponíveis foram escolhidos para comparação. A análise de DRX dos pós sintetizados de 3Y-TZP revelou a cristalização da fase tetragonal, enquanto ambos os sistemas comerciais mostraram a coexistência das fases monoclínica e tetragonal. A análise de MEV mostrou que os pós tratados termicamente a 800ºC consistem em nanopartículas esféricas aglomeradas. A morfologia dos sistemas comerciais também revelou partículas esféricas nanométricas. Os resultados revelaram que o MPP produziu cerâmicas com propriedades estruturais e morfológicas comparáveis às cerâmicas odontológicas reforçadas disponíveis comercialmente.

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18/10/2020

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PRADO, F. S. .; SIMÕES, T. C.; GONZÁLEZ, A. H. M. . Síntese e caracterização de uma cerâmica dentária experimental 3Y-TZP preparada pelo método de precursores poliméricos. Research, Society and Development, [S. l.], v. 9, n. 10, p. e7919109123, 2020. DOI: 10.33448/rsd-v9i10.9123. Disponível em: https://rsdjournal.org/index.php/rsd/article/view/9123. Acesso em: 21 jul. 2024.

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